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Standard and Microscale Experiments in General Chemistry

by: Bishop, Carl B.; Bishop, Muriel B.; Whitten, Kenneth W.

Standard and Microscale Experiments in General Chemistry

by: Bishop, Carl B.; Bishop, Muriel B.; Whitten, Kenneth W.

ISBN 13:
9780534424572
ISBN 10:
0534424570
Edition: 5th
Format: Paperback
Copyright: 05/08/2003
Publisher: Cengage Learning

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Summary

This comprehensive lab manual contains a wide array of experiments without sacrificing organizational clarity and includes categories on Energy, Kinetics, and Equilibrium. All experiments have undergone significant testing before being finalized, and many microscale experiments have been added to allow for more efficient and cost-effective means of conducting experiments.

Preface

To the Laboratory Instructor

To the Student

vii

Acknowledgments

Table of Contents

LABORATORY TECHNIQUES

(28)

Handling Chemicals

(2)

Solids

(1)

Liquids

(2)

Determination of Mass and Weight

(2)

Triple-Beam and Platform Balances

(1)

Toploading Balances

(2)

Volumetric Techniques---The Measurement of Volume

(5)

Macroscale Techniques

(1)

Graduated Cylinders

(1)

Volumetric Pipets

(2)

Burets and Titration Procedures

(1)

Volumetric Flasks

(1)

Microscale methods

(1)

Construction of Stretch Stem Micropipets

(2)

Laboratory Gas Burner

(1)

Heating and Evaporating Liquids

(1)

Separation Techniques

(3)

Gravity Filtration

(2)

Vacuum Filtration

(1)

Use of Centrifuges

(1)

Ignition of Crucible and Precipitates

(1)

Working and Handling Glass

(3)

Cutting Glass

(1)

Fire Polishing Glass

(1)

Bending Glass

(1)

Inserting Glass Tubing, Thermometers, and Funnel Stems into Corks and Rubber Stoppers

(1)

Collecting Gases

(2)

Testing for Odor

(1)

Collection of Gases

(1)

An Improvised Fume Hood

(1)

Spectrophotometer

(1)

Calibration and Use of Spectrophotometer

(1)

Measurement of Sample

(1)

Treatment of Experimental Data

(1)

Significant Figures and Calculations

(1)

Report Average Values

(1)

pH Meter

(1)

Melting and Boiling Determination

(6)

Melting Point Determination

(1)

Boiling Point Determination

(1)

EQUIPMENT

Common Laboratory Safety Equipment

(1)

Common Glassware Equipment

(1)

Common Equipment

(2)

CHEMICAL SAFETY AND LABORATORY RULES

(4)

Laboratory Safety Quiz

(2)

EXPERIMENTS

Micro Experiments

Background: Review of Simple Mathematics (Experiment 1)

(10)

Density of Solids and Liquids: Mass/Volume Measurements

(12)

Indirect Gravimetric Determination of a Hydrated Compound in a Mixture

(8)

Percent Copper and Formula Weight of a Copper Compound

(8)

Background: Solutions, Solubility and Separation Techniques

(2)

Solubilities

(10)

Separation of the Components of a Mixture

(8)

Chromatography

(10)

Background: Chemical Reactions in Aqueous Solutions and Syntheses

103

(4)

Hydrogen Ions, pH and Indicators

107

(10)

Identify Eight Metal Ions by Reactions with Anions

117

(14)

Identify Ten Inorganic Compounds by Their Inter-Chemical Reactions

131

(12)

The Formula of a Precipitated Compound

143

(12)

A Sequence of Chemical Reactions

155

(14)

Synthesis of a Compound (Alum) from Scrap Aluminum

169

(8)

Background: Periodic Table and Periodicity

177

(2)

Molecular Models: Lewis Dot Formulas, VSEPR Theory, and Valence Bond Theory

179

(14)

Chemical Periodicity of the Halide Ions

193

(10)

Relative Reactivity of Metals and the Activity Series

203

(12)

Background: Mole, Molecular Weight and Gas Laws

215

(2)

Indirect Determination of the Masses of Pieces of Magnesium

217

(8)

Density of Gases

225

(10)

The Molecular Weight of a Volatile Compound

235

(8)

Standard Molar Volume of a Gas

243

(8)

Colligative Properties

The Molecular Weight of a Compound by Freezing Point Depression Measurements

251

(8)

Background: Acids-Bases

259

(6)

Acid Base Titration Curves Using: I. an Indicator Color-Reference II. a Micro-pH Meter (micro-scale)

265

(22)

Acid Base Titrations: Analysis of Acid Solutions of Unknown Concentrations (Macro-scale)

287

(12)

Action of Antacid Tablets

299

(12)

Background: Reduction-Oxidation Reactions

311

(2)

Voltaic and Electrolytic Cells

313

(14)

Reduction-Oxidation Titrations (both micro & macro)

327

(14)

Background: Energy

341

(2)

Heat Energy Associated with Chemical and Physical Changes

343

(14)

Heats of Neutralization and Hess' Law

357

(18)

Background: Kinetics

375

(2)

Factors that Influence the Rates of Reaction

377

(10)

Rates of Chemical Reactions

387

(12)

Background: Equilibrium

399

(2)

Chemical Equilibrium---An Introduction

401

(14)

Spectrophotometric Determination of an Equilibrium Constant

415

(12)

The Spectrophotometric Determination of the Formula for a Complex Species

427

(14)

Solubility Products of Insoluble Salts

441

(12)

Determination of Ka from Measurements of pH

453

(18)

Background: Descriptive Chemistry

471

(2)

Oxygen and Some Oxides

473

(12)

Nitrogen and Its Compounds

485

(12)

The Anions of Sulfur

497

(10)

Background: Introduction to Organic Chemistry

507

(2)

Organic Qualitative Analysis

509

(14)

Commercial Esters---Aspirin and Oil of Wintergreen

523

(10)

Polymers

533

(12)

Preparation and Properties of Soaps: Properties of Detergents

545

APPENDICES

A Logarithms and pH

B Formulas, Ionic Charges and Names for Some Common Ions

C Classification of Acids

D Classification of Bases

E Solubility Rules for Common Inorganic Compounds

F Vapor Pressure of Water Near Room Temperature

G Molecular and Ionic Chemical Equations

H Concentrations and Primary Standards

I Units of Measurement

Amazon no longer offers textbook rentals. We do!

Standard and Microscale Experiments in General Chemistry

Standard and Microscale Experiments in General Chemistry

9780534424572

0534424570

Summary

Table of Contents

Supplemental Materials

Write a Review

Amazon no longer offers textbook rentals. We do!

Standard and Microscale Experiments in General Chemistry

Standard and Microscale Experiments in General Chemistry

9780534424572

0534424570

Summary

Table of Contents

Supplemental Materials

Write a Review

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