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Practical Instrumental Analysis : Methods, Quality Assurance and Laboratory Management

ISBN: 9783527329519 | 352732951X

Edition: 2nd
Format: Paperback
Publisher: Wiley-VCH
Pub. Date: 12/26/2012

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Summary Table of Contents Author Biography

The essential practical guide for analytical chemists working in industry, covering all the common methods used in industrial analytical labs. The author has a background in industry as well as extensive experience in teaching this topic, so he knows the field from the inside and can explain the contents in an easily understandable way. The first part of the book introduces the basic theoretical aspects of instrumental analysis, while the second consists of experiments that are structured as projects to be carried out by a team, thus guiding th... MOREe reader into thinking like an industrial analytical chemist. As a result, readers learn how to work efficiently, safely and accurately in an industrial setting.

This practical book in instrumental analytics conveys an overview of important methods of analysis and enables the reader to realistically learn the (principally technology-independent) working techniques the analytical chemist uses to develop methods and conduct validation. What is to be conveyed to the student is the fact that analysts in their capacity as problem-solvers perform services for certain groups of customers, i.e., the solution to the problem should in any case be processed in such a way as to be ?fit for purpose?. The book presents sixteen experiments in analytical chemistry laboratory courses. They consist of the classical curriculum used at universities and universities of applied sciences with chromatographic procedures, atom spectrometric methods, sensors and special methods ( e.g. field flow fractionation , flow injection analysis and N-determination according to Kjeldahl). The carefully chosen combination of theoretical description of the methods of analysis and the detailed instructions given are what characterizes this book. The instructions to the experiments are so detailed that the measurements can, for the most part, be taken without the help of additional literature. The book is complemented with tips for effective literature and database research on the topics of organisation and the practical workflow of experiments in analytical laboratory, on the topic of the use of laboratory logs as well as on writing technical reports and grading them (Evaluation Guidelines for Laboratory Experiments). A small introduction to Quality Management, a brief glance at the history of analytical chemistry as well as a detailed appendix on the topic of safety in analytical laboratories and a short introduction to the new system of grading and marking chemicals using the "Globally Harmonized System of Classification and Labelling of Chemicals (GHS)", round off this book. This book is therefore an indispensable workbook for students, internship assistants and lecturers (in the area of chemistry, biotechnology, food technology and environmental technology) in the basic training programme of Analytics at universities and universities of applied sciences.

Preface to the German Edition XV

Preface to the English Edition XIX

Dedication XXI

Foreword XXIII

1 Introduction 1

1.1 Analytical Chemistry – The History 1

1.2 Analytical Chemistry and Its Role in Today’s Society 2

2 Introduction to Quality Management 5

2.1 Historical Background 5

2.2 Variability 6

2.3 The Four Pillars of Wisdom (from Shewhart to Deming) 10

2.4 Zero-Defect Tolerance 10

2.5 Why Standards? 11

2.6 The Controlled Process 11

... MORE

After his apprentiship, Sergio Petrozzi worked as a chemical lab technician at the Laboratory of Physical Chemistry ETHZ (Swiss Federal Institute of Technology) and at the Swiss Federal Institute of Aquatic Sciences and Technology (EAWAG), Switzerland. After acquiring his federal diploma (Diplom H?here Fachpr?fung), he joined the Institute of Chemical Engineering ETHZ where he gained great experience as teaching assistant in laboratory courses. His daily routine focused among other topics,on the following topics at the ETHZ in Zurich: Development, optimisation and validation of analytical methods. He subsequently worked as an application chemist at B?chi Labortechnik AG, Flawil (Switzerland) with a focus on the validation of applications for environmental determinations. He has authored numerous publications in international journals and is presently employed as a Scientific Associate at the Zurich University of Applied Sciences ZHAW, W?denswil (Switzerland), where, among other things, he is teaching adviser in analytical chemistry laboratory at the Institute for Chemistry and Biological Chemistry (ICBC).

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