Multiscale Operational Organic Chemistry Vol. 2 : A Problem Solving Approach to the Laboratory
ISBN: 9780132413756 | 0132413752
Edition: 2ndFormat: Hardcover
Publisher: Prentice Hall
Pub. Date: 4/9/2008
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This comprehensive lab companion provides enough theory to help students understand how and why an operation works, but emphasizes the practical aspects of an operation to help them perform the operation successfully in the lab. The Second Edition makes substantive revisions of many operations to clarify existing material and add new information. More environmentally friendly (i.e. "green") lab experiments are encouraged. Ideal for professors who write their own lab experiments or would like custom labs but need a source for lab operations and ... MORE
| Please note this is the 1st edition Table of Contents | |
| Preface | |
| Introduction | |
| MASTERING THE OPERATIONS | |
| Learning Basic Operations | |
| The Effect of pH on a Food Preservative | |
| Extraction and Evaporation | |
| Separating the Components of ldquo;Panacetin.rdquo; | |
| Recrystallization and Melting-Point Measurement | |
| Identify... MORE | |
| Heating under Reflux | |
| Synthesis of Salicylic Acid from Wintergreen Oil | |
| Simple Distillation, Gas Chromatography | |
| Preparation of Synthetic Banana Oil | |
| Fractional Distillation | |
| Separation of Petroleum Hydrocarbons | |
| Addition, Mixing, Sublimation | |
| Preparation of Camphor | |
| Boiling Point, Refractive Index | |
| Identification of a Petroleum Hydrocarbon | |
| Column Chromatography, UV-VIS Spectrometry | |
| Isolation and Isomerization of Lycopene from Tomato Paste | |
| Steam Distillation, Infrared Spectrometry | |
| Isolation and Identification of the Major Constituent of Clove Oil | |
| Thin-Layer Chromatography, NMR Spectrometry | |
| Identification of Unknown Ketones | |
| Vacuum Distillation, Optical Rotation | |
| Optical Activity of hellip;a-Pinene | |
| Correlated Laboratory Experiments | |
| Investigation of a Chemical Bond by Infrared Spectrometry | |
| Properties of Common Functional Groups | |
| Thin-Layer Chromatographic Analysis of Drug Components | |
| Separation of an Alkane Clathrate | |
| Isomers and Isomerization Reactions | |
| Structures and Properties of Stereoisomers | |
| Bridgehead Reactivity in an S n 1 Solvolysis Reaction | |
| Reaction of Iodoetane with Saccharin, an Ambident Nucleophile | |
| Dehydration of Methylcyclohexanols | |
| Synthesis of 7,7-Dichloronorcarane Using a Phase-Transfer Catalyst | |
| Stereochemistry of the Addition of Bromine totrans-Cinnamic Acid | |
| Preparation of Bromotriphenylmethane and the Trityl Free Radical | |
| Chain-Growth Polymerization of Styrene and Methyl Methacrylate | |
| Synthesis of Ethanol by Fermentation | |
| Reaction of Butanols with Hydrobromic Acid | |
| Borohydride Reduction of Vanillin to Vanillyl Alcohol | |
| Synthesis of Triphenylmethanol and the Trityl Carbocation | |
| Identification of a Conjugated Diene from Eucalyptus Oil | |
| Spectral Identification of Terpenoids | |
| Synthesis | |
| Table of Contents provided by Publisher. All Rights Reserved. |
John W. Lehman received his Ph.D. in chemistry from the University of Colorado in Boulder. He has taught chemistry for 35 years at Lake Superior State University, a small university in Michigan's scenic Upper Peninsula. In recognition of his teaching skills, he received the State of Michigan's Teaching Excellence Award in 1990. In 2001 he funded a chemistry scholarship to help bring outstanding students into the chemistry program at Lake Superior State University. His groundbreaking lab text, Operational Organic Chemistry, was first published in 1981, and he has written three additional books for the organic chemistry laboratory.
