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The Organic Chemistry Lab Survival Guide

by: Zubrick, James W.

The Organic Chemistry Lab Survival Guide

by: Zubrick, James W.

ISBN 13:
9780471387329
ISBN 10:
0471387320
Format: Paperback
Copyright: 08/01/2000
Publisher: John Wiley & Sons Inc
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Summary

A paperback guide to the basic techniques of the organic chemistry lab. Zubrick includes practical lab advice presented with clarity and humor. The book describes the instruments and techniques used in organic chemistry lab. Diagrams show the reader how to make measurements, set up labs and perform meaningful experiments.

Safety First, Last, and Always

(8)

Accidents Will Not Happen

(1)

Disposing of Waste

(4)

Mixed Waste

(2)

Keeping a Notebook

(11)

A Technique Experiment

(3)

Notebook Notes

(2)

A Synthesis Experiment

(6)

Notebook Notes

(4)

The Acid Test

(1)

Interpreting a Handbook

(13)

CRC Handbook

(4)

Entry: 1-Bromobutane

(2)

Entry: Benzoic Acid

(2)

Lange's

(2)

Entry: 1-Bromobutane

(1)

Entry: Benzoic Acid

(1)

Merck Index

(3)

Entry: 1-Bromobutane

(3)

Entry: Benzoic Acid

(1)

The Aldrich Catalog

(3)

Entry: 1-Bromobutane

(1)

Entry: Benzoic Acid

(1)

Not Clear-Clear?

(1)

Info on the Internet

(1)

Jointware

(12)

Stoppers with Only One Number

(1)

Another Episode of Love of Laboratory

(2)

Hall of Blunders and Things Not Quite Right

(4)

Round-Bottom Flasks

(1)

Columns and Condensers

(1)

The Adapter with Lots of Names

(2)

Forgetting the Glass

(1)

Inserting Adapter Upside Down

(1)

Inserting Adapter Upside Down sans Glass

(1)

Greasing the Joints

(2)

To Grease or Not to Grease

(1)

Preparation of the Joints

(1)

Into the Grease Pit

(1)

Storing Stuff and Sticking Stoppers

(1)

Corking a Vessel

(2)

The Cork Press

(1)

The O-Ring & Cap Branch Out

(1)

Microscale Jointware

(11)

Microscale: A Few Words

(1)

Uh-Oh Rings

(1)

The O-Ring Cap Seal

(2)

Sizing Up the Situation

(1)

Why I Don't Really Know How Vacuum Tight These Seals Are

(1)

The Comical Vial (That's Conical!)

(4)

The Conical Vial as Vial

(1)

Packaging Oops

(1)

Tare to the Analytical Balance

(1)

The Electronic Analytical Balance

(1)

Heating These Vials

(1)

The Microscale Drying Tube

(1)

Gas Collection Apparatus

(4)

Generating the Gas

(2)

Isolating the Product

(1)

Other Interesting Equipment

(2)

Pipet Tips

(6)

Pre-preparing Pasteur Pipets

(3)

Calibration

(1)

Operation

(1)

Amelioration

(2)

Pipet Cutting

(1)

Pipet Filtering-Liquids

(1)

Pipet Filtering-Solids

(2)

Syringes, Needles, and Septa

(3)

The Rubber Septum

(1)

Clean and Dry

(2)

Drying Your Glassware When You Don't Need To

(1)

Drying Your Glassware When You Need To

(1)

Drying Agents

(3)

Typical Drying Agents

(1)

Using a Drying Agent

(1)

Following Directions and Losing Product Anyway

(1)

Drying Agents: Microscale

(1)

On Products

(2)

Solid Product Problems

(1)

Liquid Product Problems

(1)

The Sample Vial

(1)

Hold It! Don't Touch That Vial

(1)

The Melting Point Experiment

(16)

Sample Preparation

(2)

Loading the Melting Point Tube

(1)

Closing Off Melting Point Tubes

(1)

Melting Point Hints

(1)

The Mel-Temp Apparatus

(1)

Operation of the Mel-Temp Apparatus

(3)

The Fisher-Johns Apparatus

(1)

Operation of the Fisher-Johns Apparatus

(1)

The Thomas-Hoover Apparatus

(2)

Operation of the Thomas-Hoover Apparatus

(3)

Using the Thiele Tube

(4)

Cleaning the Tube

(1)

Getting the Sample Ready

(2)

Dunking the Melting Point Tube

(1)

Heating the Sample

(2)

Recrystallization

(15)

Finding a Good Solvent

(1)

General Guidelines for a Recrystallization

(1)

Gravity Filtration

(3)

The Buchner Funnel and Filter Flask

(2)

Just a Note

(1)

The Hirsch Funnel and Friends

(1)

Activated Charcoal

(1)

The Water Aspirator: A Vacuum Source

(2)

The Water Trap

(1)

Working with a Mixed-Solvent System---The Good Part

100

(1)

The Ethanol-Water System

100

(1)

A Mixed-Solvent System---The Bad Part

101

(1)

Salting Out

101

(1)

World Famous Fan-Folded Fluted Paper

102

(2)

Recrystallization: Microscale

104

(6)

Isolating the Crystals

105

(1)

Craig Tube Filtration

105

(3)

Centrifuging the Craig Tube

108

(2)

Getting the Crystals Out

109

(1)

Extraction and Washing

110

(13)

Never-Ever Land

111

(1)

Starting an Extraction

111

(1)

Dutch Uncle Advice

112

(1)

The Separatory Funnel

113

(3)

The Stopper

113

(1)

The Glass Stopcock

114

(1)

The Teflon Stopcock

115

(1)

The Stem

116

(1)

Washing and Extracting Various Things

116

(1)

How to Extract and Wash What

117

(6)

The Road to Recovery---Back-Extraction

118

(1)

A Sample Extraction

118

(2)

Performing an Extraction or Washing

120

(2)

Extraction Hints

122

(1)

Extraction and Washing: Microscale

123

(3)

Mixing

123

(1)

Separation: Removing the Bottom Layer

123

(1)

Separation: Removing the Top Layer

124

(2)

And Now---Boiling Stones

126

(1)

Sources of Heat

127

(8)

The Steam Bath

127

(1)

The Bunsen Burner

128

(2)

Burner Hints

129

(1)

The Heating Mantle

130

(2)

Proportional Heaters and Stepless Controllers

132

(3)

Clamps and Clamping

135

(9)

Clamping a Distillation Setup

137

(4)

Clipping a Distillation Setup

141

(3)

Distillation

144

(23)

Distillation Notes

145

(3)

Simple Distillation

145

(1)

Sources of Heat

146

(1)

The Three-Way Adapter

146

(1)

The Distilling Flask

146

(1)

The Thermometer Adapter

147

(1)

The Ubiquitous Clamp

147

(1)

The Thermometer

147

(1)

The Condenser

147

(1)

The Vacuum Adapter

148

(1)

The Receiving Flask

148

(1)

The Ice Bath

148

(1)

The Distillation Example

148

(1)

The Distillation Mistake

149

(13)

Vacuum Distillation

150

(1)

Pressure Measurement

150

(2)

Manometer Hints

152

(1)

Leaks

152

(1)

Pressure and Temperature Corrections

153

(2)

Vacuum Distillation Notes

155

(3)

Fractional Distillation

158

(1)

How This Works

158

(3)

Fractional Distillation Notes

161

(1)

Azeotropes

162

(2)

Steam Distillation

162

(1)

External Steam Distillation

162

(1)

Internal Steam Distillation

163

(1)

Steam Distillation Notes

164

(3)

Microscale Distillation

167

(4)

Like the Big Guy

167

(1)

Simple Distillation

167

(1)

Vacuum Distillation

167

(1)

Fractional Distillation

168

(1)

Steam Distillation

168

(1)

Microscale Distillation II: The Hickman Still

168

(3)

The Hickman Still Setup

168

(1)

Hickman Still Heating

169

(1)

Recovering Your Product

170

(1)

Reflux & Addition

171

(7)

Standard Reflux

171

(1)

A Dry Reflux

172

(2)

Addition and Reflux

174

(4)

Funnel Fun

174

(1)

How to Set Up

175

(3)

Reflux: Microscale

178

(2)

Addition and Reflux: Microscale

178

(2)

Sublimation

180

(2)

Microscale Boiling Point

182

(3)

Microscale BP

182

(1)

Ultramicroscale BP

183

(2)

Chromatography: Some Generalities

185

(3)

Adsorbents

185

(1)

Separation or Development

185

(1)

The Eluatropic Series

186

(2)

Thin-Layer Chromatography: TLC

188

(11)

Preparation of TLC Plates

188

(2)

Pre-prepared TLC Plates

189

(1)

The Plate Spotter

190

(1)

Spotting the Plates

190

(1)

Developing a Plate

191

(2)

Visualization

193

(1)

Interpretation

193

(2)

Multiple Spotting

195

(1)

Cospotting

196

(1)

Amazon no longer offers textbook rentals. We do!

The Organic Chemistry Lab Survival Guide

The Organic Chemistry Lab Survival Guide

9780471387329

0471387320

Summary

Table of Contents

Supplemental Materials

Write a Review

Amazon no longer offers textbook rentals. We do!

The Organic Chemistry Lab Survival Guide

The Organic Chemistry Lab Survival Guide

9780471387329

0471387320

Summary

Table of Contents

Supplemental Materials

Write a Review

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